Download Crystallization Processes in Fats and Lipid Systems by Nissim Garti, Kiyotaka Sato PDF

By Nissim Garti, Kiyotaka Sato

Participants in pharmaceutical sciences, chemistry, nutrition technological know-how, and biology evaluation rising options, techniques, and mechanisms in fats crystallization and polymorphism of recent fat, advanced blends of area of expertise fat, fatty acids, non-saponifiable lipids, and mono- and diglycerides. a few issues contain interfacial crystallization in emulsions and microemulsions, lyotropic liquid crystals and different self-assembled constructions, and crystallization in constrained volumes. different themes contain polymorphism and section transitions of fatty acids and acylglycerols, fats crystal networks, crystallization houses of cocoa butter, and separation and crystallization of oleaginous elements in cosmetics. Garti is professor of chemistry and head of the Casali Institute of utilized Chemistry on the Hebrew collage of Jerusalem, Israel. Sato teaches utilized organic technology at Hiroshima college, Japan.

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Extra info for Crystallization Processes in Fats and Lipid Systems

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The occurrence, during the growth, of faces that cannot exist on the equilibrium crystal form involves some critical σ v value. Kern [59,60] experimentally showed that ionic crystals of NaCl type change their habit when σ v exceeds a certain critical value. Here the K faces, like (111), are not stable due to their too high surface energy. However, surface reconstruction and very strong water adsorption allow these faces, not only to appear, but even to dominate growth habits. Water adsorption plays a fundamental role in determining the growth habit of sucrose crystals, on which it stabilizes the {101} stepped form through a S → F character transition.

The two interlaced spirals are mutually rotated nearly 90° and reveal that a screw dislocation crossing the (001) face of a monoclinic crystal over which a twinned layer has been crystallized promoted the lateral growth of both individuals (regular and twinned) so as to generate a periodic polysynthetic twin as illustrated in Fig. 9. 2. Polytypes Though the concept of polytypism was historically applied first to minerals and synthetic inorganic crystals, here we deal only with some examples relevant to the subject of this book.

Thermodynamics effects. The thermodynamic parameter of interest in 2D nucleation and spiral growth is the edge free energy ρ of the edges running on the adsorbing face. By assuming (a) a Langmuir-type isotherm Γ A ϭ bx A , where Γ A and x A are the edge concentration of adsorbed additive and its mole fraction in solution, respectively, and (b) an equilibrium between the impurity A adsorbed on the step and the bulk phase, when µ A ϭ µ°A ϩ kT ln xA , we can write the variation of the step free energy as ρ A ϭ ρ Ϫ kT ln x A.

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